TEKNOLOGI EKSTRAKSI FLUIDA SUPERKRITIS DAN MASERASI PADA ZINGIBER OFFICINALLE ROSCOE : AKTIVITAS ANTIOKSIDAN DAN KANDUNGAN FITOKIMIA

Authors

  • Dewi Sondari Pusat Penelitian Kimia (P2K) - LIPI
  • Eka Dian Puspitasari Pusat Penelitian Kimia (P2K) - LIPI

DOI:

https://doi.org/10.17146/jsmi.2017.18.2.4168

Keywords:

Ekstraksi CO2 superktritis, Rendemen, Zingiber officinale Rosc, Flavonoid, Phenol

Abstract

TEKNOLOGI EKSTRAKSI FLUIDA SUPERKRITIS DAN MASERASI PADA ZINGIBER OFFICINALLE ROSCOE : AKTIVITAS ANTIOKSIDAN DAN KANDUNGAN FITOKIMIA. Proses ekstraksi Zingiber officinale Roscoe denganmetode fluida superkritis dan metodemaserasi sebagai pembanding telah dilakukan. Ekstraksi CO2 superkritis dilakukan pada kondisi proses tekanan 12-16 MPa, suhu 20-40 oC, waktu ekstraksi 2-6 jam dan laju alir fluida CO2 superkritis 5,5 mL/menit. Pengaruh proses ekstraksi terhadap rendemen, aktivitas antioksi dan dan kandungan fitokimia dari Zingiber officinale Rosc telah diteliti. Hasil penelitian ekstrak kasar jahe menunjukkan bahwa rendemen tertinggi 2,99 mg/g diperoleh pada suhu 40 oC, tekanan 16 MPa dan waktu ekstraksi 6 jam, dengan kandungan fenol total 72,73 mg GEA/g ekstrak, flavonoid total 0,90 % (b/b) dan aktivitas antioksidan sebesar 63,66 μg/mL. Hasil ekstrak kasar jahe dengan metode maserasi dihasilkan rendemen 3,10 mg/g, dengan kandungan phenol total 76,68 mg GEA/g ekstrak, flavonoid total 1,18 % (b/b) dan aktivitas antioksidan sebesar 122,85 μg/mL.

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References

. M.Amir,A. Khan, M. Mujeeb,A.Ahmad, S. Usmani and M.Akhta. “PhytochemicalAnalysis and in Vitro Antioxidant Activity of Zingiber officinale.” Free Radicals and Antioxidants, vol.1, no. 4, pp. 75-81, 2011.

. O. Babova, A. Occhipinti, A. Capuzzo and M.E. Maffei. “Extraction of Bilberry (Vaccinium Myrtillus) Antioxidants Using Supercritical/

Subcritical CO2 and Ethanol as Co-Solvent.” Journal of Supercritical Fluids, vol. 107, pp. 358-363, 2016.

. Y. Bellik.” Total Antioxidant Activity And Antimicrobial Potency Of The Essential Oil And Oleoresin Of Zingiber Officinale Roscoe.” Asian Pacific Journal Tropical Disease, vol.4, no. 1, pp. 40-44, 2014.

. M.C. Mesomo, M.L. Corazza, P.M. Ndiaye, O.R.D. Santa, L. Cardozo andA.D.P. Scheer. “Supercritical CO2 ExtractsAnd Essential Oil Of Ginger (Zingiber Officinalle R.): Chemical composition and antibacterial activity.” The Journal of Supercritical Fluids, vol. 80, pp. 44-49, 2013.

. Q.Deng, K.G. Zinoviadou, C.M. Galanakis, V. Orlien, N. Grimi, E.ne Vorobiev, N. Lebovka and F.J. Barba. “The Effects Of Conventional And

Nonconventional Processing On Glucosinolates And Its Derived Forms, Isothiocyanates: Extraction, Degradation,And Applications.” Food Engeenering Review, vol. 7, no. 3, pp. 357-381, 2015.

. I.R Kubra, K. Devender and L.J. Mohan.” Effect Of Microwave-Assisted Extraction On The Release Of Polyphenols From Ginger (Zingiber Officinale).” International Journal of Food Science and Technology, vol. 48, pp. 1828-1833, 2013.

. J. Hu, Z. Guo, M. Glasius, K. Kristensen, L. Xiao and X. Xu. “Pressurized Liquid Extraction Of Ginger (Zingiber Officinale Roscoe) With Bioethanol: An Efficient And Sustainable Approach.” Journal of ChromatographyA, vol. 1218, pp. 5765-5773, 2011.

. T. Moslavac, S. Jokic, D. Subaric,K.Aladi, J. Vukoja and N. Prce”. Pressing and Supercritical CO2 Extraction of Camelina Sativa Oil”. Industrial Crops and Products, vol. 54, pp. 122-129, 2014.

. K. Czaikoski, M.C. Mesomo, R.L. Kruger, C.L. Queiroga and M.L. Corazza. “Extraction Of Campomanesia Xanthocarpa Fruit Using

Supercritical CO2 and Bioactivity Assessments.” The Journal of Supercritical Fluids, vol. 98, pp. 79-85, 2015.

. F. Bashipour and S.M. Ghoreishi.” Response Surface Optimization of Supercritical CO2 Extraction of α-Tocopherol from Gel and Skin of Aloe Vera and Amond Leaves.” The Journal of Supercritical Fluids, vol. 95, pp. 348-354, November 2014.

. N.B. Rahal, F.J. Barba, D. Barth and I. Chevalot. “Supercritical CO2 Extraction of Oil, Fatty Acids and Flavonolignans from Milk Thistle Seed: Evaluation of Their Antioxidant and Cytotoxic Activities in CaCO2 Cells”. Food and Chemical Toxicology, vol. 83, pp. 275-282, September 2015.

. K.C. Zancan, M.O.M. Marques, A.J. Petenate and M.A.A. Meireles.” Extraction Of Ginger (Zingiber Officinale Roscoe) Oleoresin With CO2 And CoSolvents: A Study Of The Antioxidant Action Of The Extracts.” Journal of Supercritical Fluids, vol. 24, pp. 57-76, 2002.

. Harwoko, S. Pramono and A.E. Nugroho.” Triterpenoid Fraction Of Centella Asiatica Leaves And In Vivo Antihypertensive Activity.” International Food Research Journal, vol. 21, pp. 149-154,2014.

. M.C. Mesomo,AdP. Scheer, E. Perez, P.M. Ndiaye and M.L. Corazza. “Ginger Zingiber Officinale R Extracts Obtained Using Supercritical CO2 and Compressed Propane- Kinetics And Antioxidant Activity Evaluation.” Journal of Supercritical Fluids, vol. 71, pp. 102-109, 2012.

. K.L. Nagendra chari, D. Manasa, P. Srinivas and H.B. Sowbhagya.” Enzyme-Assisted Extraction Of Bioactive Compounds From Ginger (Zingiber Officinale Roscoe).” Food Chemistry, vol. 139, pp. 509-514, 2013.

. F. Pourmorad, S.J. Hosseinimehr and N. Shahabimajd.” Antioxidant Activity, Phenol And Flavonoid Contents Of Some Selected Iranian

Medicinal Plants.” African Journal of Biotechnology, vol. 5, no. 11, pp. 1142-1145, 2006.

. B. Sultana, F. Anwar and M. Ashraf.” Effect Of Extraction Solvent/Technique On The Antioxidant Activity Of Selected Medicinal Plant Extracts.” Molecules, vol. 14, pp. 2167-2180, 2009.

. G. Oboh, A.J. Akinyemi and A.O. Ademiluyi. “Antioxidant And Inhibitory Effect Of Red Ginger (Zingiber Officinale Var. Rubra)And White Ginger (Zingiber Officinale Roscoe) on Fe2+ Induced Lipid Peroxidation In Rat Brain In Vitro.” Toxikologische Pathologie, vol. 64, no. 1-2, pp. 31-36, 2012.

. M. Jun, Y. Fu, J. Hong, X. Wan, C. Yang and C. Ho. “Comparison of Antioxidant Activities of Isoflavones from Kudzu Root (Pueraria lobata

Ohwi).” Journal of Food Science, vol. 68, pp. 2117- 2122,2003.

. S. Mukherjee, N.Mandal, A. Dey and B. Mondal. “An Approach Towards Optimization Of The Extraction Of Polyphenolic Antioxidants From

Ginger (Zingiber Officinale).” Journal of Food Science and Technology, pp. 1-8, 2012.

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Published

31-01-2017

How to Cite

Dewi Sondari, & Eka Dian Puspitasari. (2017). TEKNOLOGI EKSTRAKSI FLUIDA SUPERKRITIS DAN MASERASI PADA ZINGIBER OFFICINALLE ROSCOE : AKTIVITAS ANTIOKSIDAN DAN KANDUNGAN FITOKIMIA. Jurnal Sains Materi Indonesia, 18(2), 74–80. https://doi.org/10.17146/jsmi.2017.18.2.4168

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Vol. 18 No. 2 (2017): Jurnal Sains dan Materi Indonesia

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