INVESTIGATION ON PRECIPITATIONS AND DEFECTS OFTHE Fe-24Cr-2Si-0.8Mn FERRITIC SUPER ALLOY STEEL
DOI:
https://doi.org/10.17146/jsmi.2017.18.4.4123Keywords:
Ferritic Fe-24Cr-2Si-0.8Mn Alloy, Paduan Feritik Fe-24Cr-2Si-0.8Mn, FIB, SEM, TEM, EDX, STEM, HRTEMAbstract
INVESTIGATION ON PRECIPITATIONS AND DEFECTS OF THE Fe-24Cr-2Si-0.8Mn FERRITIC SUPER ALLOY STEEL. A ferritic Fe-24Cr-2Si-0.8Mn alloy was produced from granular ferro-scrap, ferrochrome, ferrosilicon and ferromanganese in a conventional induction furnace. The alloy is dedicated for application as structure material in high temperature devices, such as nuclear reactor vessel and heat exchanger. The alloy has been verified to have high tensile strength and high resistant against corrosion. The aim of this work is to study the microstructures, chemical compositions and precipitation occurred inside grain and grain boundary of the alloy, to obtain more information of its superior physical-chemical properties. STEM-EDX mappings reveal the present of relatively large aluminum oxide, silicon carbide and high oxygen and high carbon containing precipitations on the specimens. The grains that were formed, exhibit relatively strong deformations as obviously shown by the elongated grains and sub-grains with typical high density of dislocations, even though, less mechanical treatments applied. Small porosities are also present homogeneously separated on the whole view area.
ABSTRAK
INVESTIGASI TERHADAP PENGENDAPAN DAN KERUSAKAN PADA BAJA PADUAN SUPER FERRITIC Fe-24Cr-2Si-0,8Mn. Paduan Fe-24Cr-2Si-0,8Mn feritik dihasilkan dari granular ferro-scrap, ferrochrome, ferrosilicon dan ferromanganese dalam tungku induksi konvensional. Paduan ini didedikasikan untuk aplikasi sebagai bahan struktur pada perangkat suhu tinggi seperti bejana reaktor nuklir dan heat exchanger. Paduan telah diverifikasi memiliki kekuatan tarik tinggi dan tahan terhadap korosi. Tujuan dari penelitian ini adalah untuk mendalami struktur mikro, komposisi kimia dan presipitasi yang terjadi di dalam batas butir dan butir paduan, untuk mendapatkan lebih banyak informasi sifat fisik-kimia superior. Pemetaan STEM-EDX mengungkapkan adanya oksida aluminium yang relatif besar, silikon karbida dan oksigen tinggi dan presipitasi tinggi yang mengandung karbon pada spesimen. Butiran yang terbentuk, menunjukkan deformasi yang relatif kuat seperti yang ditunjukkan oleh butiran dan sub-butiran memanjang dengan kepadatan dislokasi yang khas, walaupun sedikit mendapat perlakuan mekanik. Porositas kecil juga berada secara merata terpisah pada keseluruhan daerah yang diamati.
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