FACILE ONE POT SYNTHESIS OF HIGHLY MONODISPERSE SILICA NANOPARTICLES IN WATER BASED MEDIUM
DOI:
https://doi.org/10.17146/jsmi.2012.14.1.4638Keywords:
Silica nanoparticles, Highly monodisperse, Water based synthesis, One pot synthesisAbstract
FACILE ONE POT SYNTHESIS OF HIGHLY MONODISPERSE SILICA NANOPARTICLES
IN WATER BASED MEDIUM. Highly monodisperse silica nanoparticles (SNs) were successfully prepared
using water based synthesis. The right catalyst and controllable release of silanol compounds into water phase
was the two mostimportant parameters in the SNs water based synthesis. The particle size of the SNs
produced by this method was easily controlled by changing TetraEthyl OrthoSilicate (TEOS) concentration.
The particle size ranging from 60 nm to 200 nm can be prepared in one pot synthesis. The SNs were analyzed
by using dynamic light scattering.
Downloads
References
. GOSA, K.-L. and V. URICANU, Colloids and Surfaces A: Physicochemical and Engineering Aspects, . 197 (1-3) (2002) 257-269
. K.K. UNGER,D.KUMAR,M. GRÜN,G.BÜCHEL,
S. LÜDTKE, T. ADAM, K. SCHUMACHER, S. RENKER, Journal of Chromatography A, 892 (1-2)(2000)47-55
. G. LEDER, T. LADWIG, V. VALTER, S. FRAHN,
J. MEYER, Progress in Organic Coatings, 45 (2-3)(2002)139-144
. H.T. CHUA, K.C. NG,A. CHAKRABORTY, N.M.OO, M.A. OTHMAN, Journal of Chemical & Engineering Data, 47 (5) (2002) 1177-1181
. VATTA, L.L., J. KRAMER, and K.R. KOCH, Separation Science and Technology, 42 (9) (2007)
-2002
. STÖBER, W., A. FINK, and E. BOHN, Journal of
Colloid and Interface Science, 26 (1) (1968) 62-69
. S.KANG,S.I.HONG,C.R.CHOE,M.PARK,S.RIM,
J. KIM, Polymer, 42 (3) (2001) 879-887
. BERGNA, H.E. and W.O. ROBERTS, Colloidal
Silica Fundamentals and Applications, NewYork:
Taylor & Francis Group, LLC (2006)
. HARTEN, K.D.,A.P.T. ATHANASOPOULOS, and
V. KITAEV, Langmuir, 24 (2008) 1714-1720
. YOKOI, T., et al.,Chemistry of Materials, 21 (2009) 3719-3729
. IBRAHIM, I.A.M., A.F.F. ZIKRY, and M.A.
SHARAF, Journal of American Science, 6 (11)(2010)985-989
. T. YOKOI, Y. SAKAMOTO, O. TERASAKI, Y.
KUBOTA, T. OKUBO, T. TATSUMI, Journal of
the American Chemical Society, 128 (42) (2006)
-13665
. K.S. RAO, K. EL-HAMI, T. KODAKI, K.
MATSUSHIGE, K. MAKINO, Journal of Colloid
and Interface Science, 289 (1) (2005) 125-131
. L. SINGH, S. BHATTACHARYYA, G. MISHRA, S.
AHALAWAT, Applied Nanoscience, 1 (3) (2011) 117-122
. X.-D.WANG,Z.-X. SHEN,T. SANG,X.-B.CHENG,
M.-F. LI, L.-Y. CHEN, Z.-S. WANG, Journal of
Colloid and Interface Science, 341 (1) (2010) 23-29
. R.LINDBERG,G.R.SUNDHOLM,B.PETTERSEN,
J. SJO¨BLOM, S.E. FRIBERG,Colloidsand Surfaces
A: Physicochemical and Engineering Aspects,
-124 (0) (1997) 549-560
. KIM, K.-S., J.-K. KIM, and W.-S. KIM, Ceramics
International, 28 (2) (2002) 187-194
. M.A. SNYDER, J.A. LEE, T.M. DAVIS, L.E. SCRIVEN, M. TSAPATSIS, Langmuir, 23 (20)(2007)9924-9928
. T.M. DAVIS, M.A. SNYDER, J.E. KROHN, M.
TSAPATSIS,Chemistry of Materials, 18 (25) (2006)
-5816
. DONATTI, D. and D. VOLLET, Journal of Sol-Gel Science and Technology, 17 (1) (2000) 19-24
. PATWARDHAN, S.V. and S.J. CLARSON,
Inorg. Organomet Polym., 13 (1) (2003) 49-53
. BRAMBILLA, R., F. SILVEIRA, and J.H.Z. DOS
SANTOS, Investigating Morphological Changes
on Octadecyl Modifiedsilicas by SEM and AFM ,(2007)
. BOGUSH, G.H., M.A. TRACY, and C.F. ZUKOSKI
IV, Journal of Non Crystalline Solids, 104 (1)(1988)95-106
. G. CANTON, R. RICCO, F. MARINELLO, S.
CARMIGNATO, F. ENRICHI, Journal of
Nanoparticle Research, 13 (9) (2011) 4349-4356
Downloads
Published
How to Cite
Issue
Section
License

This work is licensed under a Creative Commons Attribution-ShareAlike 4.0 International License.





