ANALYSIS OF CRYSTAL STRUCTURE AND FUNCTIONAL GROUPS OF NiFe2O4 USING SOL GEL METHOD

Authors

  • Mashadi Pusat Teknologi Bahan Maju (PSTBM) - BATAN
  • Yunasfi Pusat Teknologi Bahan Maju (PSTBM) - BATAN
  • Wisnu Ari Adi Pusat Teknologi Bahan Maju (PSTBM) - BATAN

DOI:

https://doi.org/10.17146/jsmi.2016.17.3.4194

Keywords:

NiFe2O4, Sol gel, Crystal structure, Functional groups

Abstract

ANALYSIS OF CRYSTAL STRUCTURE AND FUNCTIONAL GROUPS OF NiFe2O4 USING SOL GEL METHOD. A synthesis and characterization NiFe2O4 with sol gel method have been conducted. Fe2(NO3)3.9H2O powder mixed with Ni(NO3)2 was dissolved in 50 ml of polyethylene glycol at room temperature, then heated at a temperature of approximately 60 °C for 1 hour while stirring to form a wet gel. The gel was then dried in an oven at 120 °C for 5 hours and grinded to form a powder NiFe2O4. NiFe2O4 powder was then heated with a furnace at a temperature variation of 400°C, 600 °C, 800 °C and 1000 °C for 5 hours respectively. X-Ray Diffraction (XRD) pattern indicates that in this stage the sample is single phase. Fourier Transform Infra Red (FT-IR) spectroscopy analysis showed two absorption bands in the range of 411 and 599 cm-1 related to octahedral and tetrahedral sites.

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Published

30-04-2016

How to Cite

Mashadi, Yunasfi, & Wisnu Ari Adi. (2016). ANALYSIS OF CRYSTAL STRUCTURE AND FUNCTIONAL GROUPS OF NiFe2O4 USING SOL GEL METHOD. Jurnal Sains Materi Indonesia, 17(3), 131–135. https://doi.org/10.17146/jsmi.2016.17.3.4194

Issue

Vol. 17 No. 3 (2016): Jurnal Sains dan Materi Indonesia

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Articles

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