Porous Carbon Black Microsphere from Palm Oil Black Liquor

Jayadi Jayadi; Akhiruddin Maddu; Yessie Sari; Wahyu Bambang Widayatno; Agus Sukarto Wismogroho; Cherly Firdarini; Marga Asta Jaya  Mulya

doi:10.55981/jsmi.2023.686

Authors

Jayadi Jayadi 1) Department of Physics, Faculty of Mathematics and Natural Sciences, IPB University, Indonesia,2) Research Centre of Advanced Material, The National Research and Innovation Agency of Indonesia, Indonesia
Akhiruddin Maddu Department of Physics, Faculty of Mathematics and Natural Sciences, IPB University, Bogor, 16680, Indonesia
Yessie Sari IPB University
Wahyu Bambang Widayatno Research Centre of Advanced Material, The National Research and Innovation Agency of Indonesia, Indonesia
Agus Sukarto Wismogroho Research Centre of Advanced Material, The National Research and Innovation Agency of Indonesia, Indonesia
Cherly Firdarini Research Centre of Advanced Material, The National Research and Innovation Agency of Indonesia, Indonesia
Marga Asta Jaya Mulya Research Centre of Optoelectronic, The National Research and Innovation Agency of Indonesia, Indonesia

DOI:

https://doi.org/10.55981/jsmi.2023.686

Keywords:

Spray Pyrolysis, Black Liquor, Carbon Black, microspheres

Abstract

The aim of this research is to synthesize porous carbon black microspheres from palm oil black liquor through an in-house spray pyrolysis system. The in-house spray pyrolysis (SP) system was developed using a horizontal furnace. To test the developed SP equipment, the temperature profiles within the developed spray pyrolysis chamber were examined at 3 different setting temperatures (800, 900, and 1000 °C). These temperatures were also applied for synthesizing the carbon black microspheres, with and without nitrogen as carrier gas. The morphology of carbon black produced by using SP equipment was tested by a 3D Optical Microscope and FE-SEM. The optimum temperature obtained in this study is 1000 ºC according to the characterization of carbon black microspheres produced. The FE-SEM analysis indicated the presence of spherical carbon having microstructures. This indicates that the in-house spray pyrolysis machine has been successfully developed for synthesizing carbon black microspheres.

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