KARAKTERISASI DAN POTENSI KATALIS KARBON AKTIF TERSULFONASI LIMBAH KAYU PADA REAKSI HIDROLISIS SEKAM PADI MENGGUNAKAN MICROWAVE
Main Article Content
Abstract
Lignocellulose biomass is a raw material for developing various promising products, such as wood waste, which can
be used as raw material for the production of activated carbon as a catalyst. This research aims to characterize activated
carbon for hydrolisis catalyst. In this study, the process of making activated carbon from mixed camphor and meranti
wood was made through pyrolysis process at temperature of 500°C, followed by sulfonation using H2
SO4
10N on
reflux. The sulfonated activated carbon product (KA-SO3
H) was then characterized according to Indonesia National
Standard (SNI) including recovery value, moisture content, ash content, fly ash, fixed carbon, iodine absorption, while
acidity and functional groups were measured using amonia adsorption and FTIR analysis, respectively. Furthermore,
the sulfonated activated carbon was tested for its application in the hydrolysis reaction of rice husks using microwave
with vary rice husk weight namely 2, 4 ,6 ,8, and 10 g at 400 and 600 W for 5, 7, and 9 minutes, respectively. The
f
iltrate was then analyzed for its glucose levels using the DNS method (Dinitrosalycilic acid). The optimum condition of
the hydrolysis reaction using sulfonated activated carbon catalyst were 400 W power, 1:8 ratio of rice husk and catalyst
in 9 minutes duration. The optimum condition produced 330.51 ppm glucose levels with glucose yield percentages was
61.97%, and required energy was 216 kJ.
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